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    Solvent-free nitration of electron-rich arenes

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    UA_deposited_Arene_Nitration_m ...
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    Description:
    Final Accepted Manuscript
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    Author
    Jagadish, Bhumasamudram
    Hurley, Nathaniel R.
    Mash, Eugene A.
    Affiliation
    Univ Arizona, Dept Chem & Biochem
    Issue Date
    2017
    Keywords
    2
    4-Dinitroanisole
    additive-free
    nitration
    solvent-free
    
    Metadata
    Show full item record
    Publisher
    TAYLOR & FRANCIS INC
    Citation
    Bhumasamudram Jagadish, Nathaniel R. Hurley & Eugene A. Mash (2017) Solvent-free nitration of electron-rich arenes, Synthetic Communications, 47:24, 2395-2398, DOI: 10.1080/00397911.2017.1378682
    Journal
    SYNTHETIC COMMUNICATIONS
    Rights
    © 2017 Taylor & Francis
    Collection Information
    This item from the UA Faculty Publications collection is made available by the University of Arizona with support from the University of Arizona Libraries. If you have questions, please contact us at repository@u.library.arizona.edu.
    Abstract
    Nitration of relatively electron-rich arenes does not require an additive or a solvent. For example, reaction on a gram scale of anisole with acetyl nitrate, generated in situ by mixing 100% HNO3 with acetic anhydride, produced 2,4-dinitroanisole in 82% yield after crystallization of the crude product. Results with five additional monosubstituted benzene derivatives possessing highly activated, weakly activated, or weakly deactivated rings are reported. [GRAPHICS] .
    Note
    12 month embargo; published online: 03 October 2017
    ISSN
    0039-7911
    1532-2432
    DOI
    10.1080/00397911.2017.1378682
    Version
    Final accepted manuscript
    Sponsors
    Strategic Environmental Research and Development Program [ER-2221]
    Additional Links
    https://www.tandfonline.com/doi/full/10.1080/00397911.2017.1378682
    ae974a485f413a2113503eed53cd6c53
    10.1080/00397911.2017.1378682
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